Reaktion #2539

ord-0f4298d191fb4ea180b3c22f289b3eb0

Reaktionsgleichung

Cc1ccc(N)cc1C
3,4-xylidine
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
→
Cc1ccc(NC(=O)c2ccc([N+](=O)[O-])cc2)cc1C
title compound
Cc1ccc(NC(=O)c2ccc([N+](=O)[O-])cc2)cc1C
4-Nitro-N-(3,4-dimethylphenyl)benzamide

Edukte

Cc1ccc(N)cc1C
3,4-xylidine
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using 3,4-xylidine (1.35 g, 11.0 mmol) and 4-nitrobenzoic acid (1.69 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 2.70 g (quantitative) of the title compound in the form of light yellow crystals.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03