Reaktion #2533

ord-225d5fd599ed478295e732ac8190f2ec

Reaktionsgleichung

Cc1ccc(N)cc1
p-toluidine
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
Cc1ccc(NC(=O)c2ccc([N+](=O)[O-])cc2)cc1
title compound
Ausbeute 99.6%
Cc1ccc(NC(=O)c2ccc([N+](=O)[O-])cc2)cc1
4-Nitro-N-(4-methylphenyl)benzamide
Ausbeute 99.6%

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using p-toluidine (1.19 g, 11.0 mmol) and 4-nitrobenzoic acid (1.77 g, 10.5 mmol), the procedure of Reference Example 16 was repeated to obtain 2.68 g (99.6%) of the title compound in the form of light yellow needle crystals.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03