Reaktion #2529

ord-0da5c45fb1f94fe58e6de013c7b3d1b3

Reaktionsgleichung

COC(=O)c1ccccc1N
methyl anthranilate
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
COC(=O)c1ccccc1NC(=O)c1ccc([N+](=O)[O-])cc1
title compound
Ausbeute 72.9%
COC(=O)c1ccccc1NC(=O)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(2-methoxycarbonylphenyl)benzamide
Ausbeute 72.9%

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using methyl anthranilate (3.02 g, 20.0 mmol) and 4-nitrobenzoic acid (3.67 g, 22.0 mmol), the procedure of Reference Example 16 was repeated to obtain 4.20 g (72.9%) of the title compound in the form of light yellow prism crystals.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03