Reaktion #2528

ord-555bc4c8dfda4c9f9927d3dfcbc0d7ef

Reaktionsgleichung

Nc1cccc([N+](=O)[O-])c1
3-nitroaniline
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
→
O=C(Nc1cccc([N+](=O)[O-])c1)c1ccc([N+](=O)[O-])cc1
title compound
Ausbeute 83.2%
O=C(Nc1cccc([N+](=O)[O-])c1)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(3-nitrophenyl)benzamide
Ausbeute 83.2%

Edukte

Nc1cccc([N+](=O)[O-])c1
3-nitroaniline
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using 3-nitroaniline (2.76 g, 16.5 mmol) and 4-nitrobenzoic acid (2.51 g, 15.0 mmol), the procedure of Reference Example 16 was repeated to obtain 3.58 g (83.2%) of the title compound in the form of light yellow crystals.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03