Reaktion #2522

ord-20a899a14e114ac08ae516cd5bce4b60

Reaktionsgleichung

Nc1ccccc1
aniline
O=C(O)c1ccc([N+](=O)[O-])cc1
4-nitrobenzoic acid
O=C(Nc1ccccc1)c1ccc([N+](=O)[O-])cc1
title compound
Ausbeute 97.5%
O=C(Nc1ccccc1)c1ccc([N+](=O)[O-])cc1
4-Nitro-N-(phenyl)benzamide
Ausbeute 97.5%

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using aniline (1.50 ml, 16.5 mmol) and 4-nitrobenzoic acid (1.77 g, 10.5 mmol), the procedure of Reference Example 16 was repeated to obtain 2.48 g (97.5%) of the title compound in the form of colorless powder.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03