Reaktion #2507846

ord-98c3198f70774fed8176f88e3b49eb54

Reaktionsgleichung

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene
→
NCC(=O)O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
Trehalose Glycine

Edukte

O.O.OC[C@H]1O[C@H](O[C@H]2O[C@H](CO)[C@@H](O)[C@H](O)[C@H]2O)[C@H](O)[C@@H](O)[C@@H]1O
trehalose dihydrate
NCC(=O)O
glycine
CC(C[*:1])[*:2]
polypropylene

Reagenzien

Keine

Lösungsmittel

O
water
O
water

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    workup.ADDITIONwas added at room temperature
  2. 2
    Sonstigewas obtained
  3. 3
    workup.ADDITIONWithout adding any acid

Vorschrift

17.84 g of trehalose dihydrate and 4.03 g of glycine were carefully weighed and transferred into a sterile polypropylene bottle, to which 300 ml of purified water was added at room temperature and stirred slowly until a clear solution was obtained. The pH was measured and found to be 5.5. Without adding any acid, the volume was adjusted to 350 ml with purified water. The pH was measured and found to be 5.5.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07956028B2uspto-grants-2011_06