Reaktion #2506

ord-df69311069264a20a142aa147b4fbb47

Reaktionsgleichung

COc1ccccc1N
o-anisidine
O=[N+]([O-])c1cccc(S(=O)(=O)Cl)c1
3-nitrobenzenesulfonyl chloride
→
COc1ccccc1NS(=O)(=O)c1cccc([N+](=O)[O-])c1
title compound
Ausbeute 89.5%
COc1ccccc1NS(=O)(=O)c1cccc([N+](=O)[O-])c1
N-(2-Methoxyphenyl)-3-nitrobenzenesulfonamide
Ausbeute 89.5%

Edukte

COc1ccccc1N
o-anisidine
O=[N+]([O-])c1cccc(S(=O)(=O)Cl)c1
3-nitrobenzenesulfonyl chloride

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Using o-anisidine (1.0 ml, 8.55 mmol) and 3-nitrobenzenesulfonyl chloride (1.95 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.36 g (89.5%) of the title compound in the form of light yellow needle crystals.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728835uspto-grants-1998_03