Reaktion #2483

Reaktionsgleichung

ethyl 3-(N-vinylformamido)propionate

allylamine

sodium methoxide

→

N-allyl-3-(N-vinylformamido)propionamide

Lösungsmittel

methanol

Reaktionsbedingungen

Vorschrift

A 100mL stainless steel high pressure reactor was charged with 17.1 grams (0.1 mol) of ethyl 3-(N-vinylformamido)propionate, 5.7 grams (0.1 mol) of allylamine and 0.15 gram of 25% sodium methoxide in methanol solution. The mixture was heated at 90° C. for 3 hours. Subsequent NMR analysis of the reaction mixture showed no conversion of the starting materials.

Quelle