Reaktion #2441736

ord-399e7e9b534c4a3db504d8db5ceb4c98

Reaktionsgleichung

CC1CCc2nc3sc4c(c3c(=O)n2CC1)CCCC4=O
compound 17
CC1CCc2nc3sc4c(c3c(=O)n2CC1)CCCC4=O
2,3,8,9,10,11-Hexahydro-9-methyl-[1]benzothieno[2′,3′: 4,5]pyrimido[1,2-a]azepine-4,13(1H,7H)-dione
O=c1c2c3c(sc2nc2ccccn12)CCCC3
using compound 25
O=c1c2c3c(sc2nc2ccccn12)CCCC3
1,2,3,4-Tetrahydro-12H-[1]benzothieno[2,3-d]pyrido[1,2-a]pyrimidin-12-one
→
O=C1CCCc2c1sc1nc3ccccn3c(=O)c21
Compound 26
O=C1CCCc2c1sc1nc3ccccn3c(=O)c21
2,3-Dihydro-12H-[l]benzothieno[2,3-d]pyrido[1,2-a]pyrimidin-4, 12(1H)-dione

Edukte

CC1CCc2nc3sc4c(c3c(=O)n2CC1)CCCC4=O
compound 17
CC1CCc2nc3sc4c(c3c(=O)n2CC1)CCCC4=O
2,3,8,9,10,11-Hexahydro-9-methyl-[1]benzothieno[2′,3′: 4,5]pyrimido[1,2-a]azepine-4,13(1H,7H)-dione
O=c1c2c3c(sc2nc2ccccn12)CCCC3
using compound 25
O=c1c2c3c(sc2nc2ccccn12)CCCC3
1,2,3,4-Tetrahydro-12H-[1]benzothieno[2,3-d]pyrido[1,2-a]pyrimidin-12-one

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Compound 26 was synthesized by the method described for compound 17 using compound 25 as a starting material.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07754709B2uspto-grants-2010_07