Reaktion #2389372

ord-f123f332bfe54ce7924d00ee0cba471b

Reaktionsgleichung

COc1ccc(CC(C)(C)NCC(O)COc2ccc(Cl)cc2)cc1.Cl
( 5 )
COc1ccc(CC(C)(C)NCC(O)COc2ccc(Cl)cc2)cc1.Cl
N-[2-Hydroxy-3-(4-chlorophenoxy)propyl]-1,1-dimethyl-2-(4-methoxyphenyl)ethylamine Hydrochloride
C=CCOCC(O)CNC(C)(C)Cc1ccc(OC)cc1
( 29 )
C=CCOCC(O)CNC(C)(C)Cc1ccc(OC)cc1
N-(2-Hydroxy-3-allyloxypropyl)-1,1-dimethyl-2-(4-methoxyphenyl)ethylamine
→
COc1ccc(CC(C)(C)NCC(O)COc2ccc(Cl)c(Cl)c2)cc1.Cl
N-[2-hydroxy-3-(3,4-dichlorophenoxy)propyl]-1,1-dimethyl-2-(4-methoxyphenyl)ethylamine Hydrochloride

Edukte

—
( 10 )
—
( 9 )
—
( 63 )
—
( 100 )
COc1ccc(CC(C)(C)NCC(O)COc2ccc(Cl)cc2)cc1.Cl
( 5 )
COc1ccc(CC(C)(C)NCC(O)COc2ccc(Cl)cc2)cc1.Cl
N-[2-Hydroxy-3-(4-chlorophenoxy)propyl]-1,1-dimethyl-2-(4-methoxyphenyl)ethylamine Hydrochloride
C=CCOCC(O)CNC(C)(C)Cc1ccc(OC)cc1
( 29 )
C=CCOCC(O)CNC(C)(C)Cc1ccc(OC)cc1
N-(2-Hydroxy-3-allyloxypropyl)-1,1-dimethyl-2-(4-methoxyphenyl)ethylamine
—
( 9 )

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

GC/EI-MS, m/z (rel. int.) 382 (M−15,0.1), 279 (10), 279 (9), 278 (63), 276 (100), 163 (9), 146 (5), 121 (29).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06432656B1uspto-grants-2002_08