Reaktion #2386279

ord-d1c06f72f25048d29e0b92563b5f21ae

Reaktionsgleichung

Cc1ccc(S(=O)(=O)O)cc1
p-toluenesulfonic acid
NC(=O)c1ccco1
Furan-2-carboxamide
CC(C)(C)C=O
pivaldehyde
c1ccc2[nH]nnc2c1
benzotriazole
→
CC(C)(C)C(NC(=O)c1ccco1)n1nnc2ccccc21
title compound
CC(C)(C)C(NC(=O)c1ccco1)n1nnc2ccccc21
N-[1-(1H-1,2,3-Benzotriazol-1-yl)-2,2-dimethylpropyl]-2-furamide

Edukte

Cc1ccc(S(=O)(=O)O)cc1
p-toluenesulfonic acid
NC(=O)c1ccco1
Furan-2-carboxamide
CC(C)(C)C=O
pivaldehyde
c1ccc2[nH]nnc2c1
benzotriazole

Reagenzien

Keine

Lösungsmittel

Cc1ccccc1C
xylene

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Furan-2-carboxamide, pivaldehyde, benzotriazole, and p-toluenesulfonic acid in xylene were processed as described in Example 18B to provide the title compound.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06495576B2uspto-grants-2002_12