Reaktion #2384790

ord-818d695750fd48489a207ea31713dae7

Reaktionsgleichung

CC1=NCCc2ccccc21
1-Methyl-3,4-dihydroisoquinoline
CI
iodomethane
→
CC1=[N+](C)CCc2ccccc21.[I-]
crystals
CC1=[N+](C)CCc2ccccc21.[I-]
1,2-Dimethyl-3,4-dihydroisoquinolinium Iodide

Edukte

CC1=NCCc2ccccc21
1-Methyl-3,4-dihydroisoquinoline
CI
iodomethane

Reagenzien

Keine

Lösungsmittel

CC(C)=O
acetone

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

1-Methyl-3,4-dihydroisoquinoline (780 mg) was dissolved in acetone (7 ml) and iodomethane (0.38 ml) added. The solution was allowed to stand overnight at room temperature. The product was obtained as pale yellow crystals (1.4 g).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06492378B1uspto-grants-2002_12