Reaktion #2383780

ord-418306255f36449a96863edfa193ae18

Reaktionsgleichung

O=C(O)c1ccccc1
Benzoic acid
C=COCCCl
2-chloroethyl vinyl ether
[Na+].[OH-]
sodium hydroxide
CCN(CC)CC
triethylamine
C=COCCOC(=O)c1ccccc1
Benzoyloxyethyl Vinyl Ether

Lösungsmittel

Reaktionsbedingungen

Temperatur
120°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Benzoic acid (244 g) (2 mol) was dissolved in 3,000 ml of toluene, and thereto were added 320 g of 2-chloroethyl vinyl ether, 88 g of sodium hydroxide, 25 g of tetrabutylammonium bromide, and 100 g of triethylamine. The resulting mixture was stirred with heating at 120° C. for 5 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06489080B2uspto-grants-2002_12