Reaktion #2383780
ord-418306255f36449a96863edfa193ae18
Reaktionsgleichung
Benzoic acid
2-chloroethyl vinyl ether
sodium hydroxide
triethylamine
→
Benzoyloxyethyl Vinyl Ether
Reagenzien
Lösungsmittel
Reaktionsbedingungen
Temperatur
120°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Vorschrift
Benzoic acid (244 g) (2 mol) was dissolved in 3,000 ml of toluene, and thereto were added 320 g of 2-chloroethyl vinyl ether, 88 g of sodium hydroxide, 25 g of tetrabutylammonium bromide, and 100 g of triethylamine. The resulting mixture was stirred with heating at 120° C. for 5 hours.