Reaktion #2383768

Reaktionsgleichung

N,N-bis-(tert-butoxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine

hydrochloric acid

→

N,N-Bis-(hydroxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine-hydrochloride

Lösungsmittel

tetrahydrofuran

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe resulting reaction mixture
2. 2
   Einengenconcentrated by evaporation in a vacuum
3. 3
   FiltrationThen, the product is filtered off
4. 4
   Sonstigedried in a medium-high vacuum

Vorschrift

1.67 g (5 mmol) of N,N-bis-(tert-butoxycarboxy-methyl)-S-ethyl-2-mercaptoethylamine is dissolved in 12 ml of tetrahydrofuran and mixed with 6 ml of concentrated hydrochloric acid. The resulting reaction mixture is stirred for 1 hour at room temperature and concentrated by evaporation in a vacuum. The residue is pulverized with 10 ml of absolute diethyl ether. Then, the product is filtered off and dried in a medium-high vacuum.

Quelle