Reaktion #2383764

Reaktionsgleichung

4-chloro-3-methylpyrazole

formalin

→

solid

Ausbeute 95.0%

N-hydroxymethyl-4-chloro-3-methylpyrazole

Ausbeute 95.0%

Lösungsmittel

methanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeWater and methanol were then evaporated

Vorschrift

116 g (1.0 mol) of 4-chloro-3-methylpyrazole in 50 ml of methanol were dissolved in 100 g (1.0 mol) of formalin solution (30%) at room temperature. Water and methanol were then evaporated. The title compound remained as a white solid (yield 95%).

Quelle