Reaktion #2376278

Reaktionsgleichung

methyl 4-alloxyphenylacetate

ortho-dichlorobenzene

→

methyl 3-allyl-4-hydroxyphenylacetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe solvent was removed under reduced pressure
2. 2
   Sonstigethe residue was purified by chromatography (silica gel, 50% methylene chloride in hexane)
3. 3
   Sonstigeto afford the tittle compound

Vorschrift

A solution of methyl 4-alloxyphenylacetate (3.1 grams) in dry ortho-dichlorobenzene (50 mL) was refluxed for 25 hours. The solvent was removed under reduced pressure, and the residue was purified by chromatography (silica gel, 50% methylene chloride in hexane) to afford the tittle compound.

Quelle