Reaktion #2373113

ord-81d2853274df44a99243bae0279f314f

Reaktionsgleichung

COC(=O)CSCc1ccc(Cl)cc1
methyl 2-(4-chlorobenzylmercapto)-acetate
NO
hydroxylamine
O=C(CSCc1ccc(Cl)cc1)NO
2-(4-Chlorobenzylmercapto)-acetohydroxamic acid

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A solution of 0.15 mol of methyl 2-(4-chlorobenzylmercapto)-acetate in 50 ml of methanol is mixed with a solution of 0.225 mol of hydroxylamine (base) and 0.15 mol of NaOH3 in 150 ml of methanol.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04325964uspto-grants-1982_04