Reaktion #2373079

Reaktionsgleichung

3-diphenylmethyl-2,3,5,6,7,8-hexahydrothiazolo[3,2-a][1,3]diazepin-3-ol

hydrochloric acid

→

desired product

3-Diphenylmethyl-2,3,5,6,7,8-hexahydrothiazolo[3,2-a][1,3]diazepin-3-ol hydrochloride

Lösungsmittel

acetone

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe resulting solid is collected by filtration

Vorschrift

A solution of 3.0 g. of 3-diphenylmethyl-2,3,5,6,7,8-hexahydrothiazolo[3,2-a][1,3]diazepin-3-ol in 30 ml. of acetone is treated with 4 ml. of 3 N ethanolic hydrochloric acid. The resulting solid is collected by filtration, giving the desired product, m.p. 205° C. (dec.).

Quelle