Reaktion #2357491

Reaktionsgleichung

2-(4-methoxy-phenylsulfanyl)-2,5-dimethyl-hex-4-enoic acid ethyl ester

→

2-(4Methoxy-phenylsulfanyl)-2,5-dimethyl-hex-4-enoic acid

Lösungsmittel

methanol

NaOH

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe resulting reaction mixture

Vorschrift

2-(4Methoxy-phenylsulfanyl)-2,5-dimethyl-hex-4-enoic acid was prepared starting from 2-(4-methoxy-phenylsulfanyl)-2,5-dimethyl-hex-4-enoic acid ethyl ester (2.0 g, 6.4 mmol) dissolved in methanol (50 ml) and 10 N NaOH (20 ml). The resulting reaction mixture was worked up as outlined in Example 1. Yield is 1.9 g, 99% of low melting solid. MS: 280 (M+H)+.

Quelle