Reaktion #2356719

ord-c0b0802a4a274e109a330d1de8d25fb9

Reaktionsgleichung

CC(C[*:1])[*:2]
polypropylene
O=C([O-])O.[Na+]
sodium hydrogen carbonate
O=C(O)CCSSCCC(=O)O
3,3′-dithiodipropionic acid
O=C([O-])CCSSCCC(=O)[O-].[Na+].[Na+]
Disodium 3,3′-Dithiodipropionate

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigedried
  2. 2
    Sonstigemelted above 225° C.

Vorschrift

A 1-liter polypropylene beaker was charged with a solution of 42 g (0.50 mole) of sodium hydrogen carbonate in 100 g of distilled water, followed by the slow addition of 52.5 g (0.25 mole) of 3,3′-dithiodipropionic acid, which required about 10 minutes. The resulting paste was spread on an evaporating tray and dried. The salt product was white-colored and melted above 225° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06329455B1uspto-grants-2001_12