Reaktion #2356719
ord-c0b0802a4a274e109a330d1de8d25fb9
Reaktionsgleichung
polypropylene
sodium hydrogen carbonate
3,3′-dithiodipropionic acid
→
Disodium 3,3′-Dithiodipropionate
Reagenzien
Keine
Lösungsmittel
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1Sonstigedried
- 2Sonstigemelted above 225° C.
Vorschrift
A 1-liter polypropylene beaker was charged with a solution of 42 g (0.50 mole) of sodium hydrogen carbonate in 100 g of distilled water, followed by the slow addition of 52.5 g (0.25 mole) of 3,3′-dithiodipropionic acid, which required about 10 minutes. The resulting paste was spread on an evaporating tray and dried. The salt product was white-colored and melted above 225° C.