Reaktion #2346907

ord-d0478842effc4fb4abf26407df9f53d6

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigecondensed in a tube
  2. 2
    SonstigeThe tube is sealed
  3. 3
    Temperaturthe reaction mixture is warmed
  4. 4
    TemperaturThe sealed tube was cooled
  5. 5
    SonstigeSolvent was evaporated
  6. 6
    Sonstigethe residue was purified by standard methods

Vorschrift

Ammonia is condensed in a tube containing 2-amino-3-(4-bromobenzoyl)benzeneacetic acid, ethyl ester. The tube is sealed and the reaction mixture is warmed. The sealed tube was cooled and opened. Solvent was evaporated and the residue was purified by standard methods to give Compound 15.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05475034uspto-grants-1995_12