Reaktion #2346907
ord-d0478842effc4fb4abf26407df9f53d6
Reaktionsgleichung
Reagenzien
Keine
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1Sonstigecondensed in a tube
- 2SonstigeThe tube is sealed
- 3Temperaturthe reaction mixture is warmed
- 4TemperaturThe sealed tube was cooled
- 5SonstigeSolvent was evaporated
- 6Sonstigethe residue was purified by standard methods
Vorschrift
Ammonia is condensed in a tube containing 2-amino-3-(4-bromobenzoyl)benzeneacetic acid, ethyl ester. The tube is sealed and the reaction mixture is warmed. The sealed tube was cooled and opened. Solvent was evaporated and the residue was purified by standard methods to give Compound 15.