Reaktion #2328127

Reaktionsgleichung

1-Iodo-2-methyl-benzene

1-Difluoromethoxy-4-ethynyl-benzene

→

title compound

1-{[4-(difluoromethoxy)phenyl]ethynyl}-2-methylbenzene

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigewas obtained as a light brown oil, (0.141 g, 79%),

Vorschrift

The title compound was prepared in substantially the same manner as described in Example 12, step 3 starting from 1-Iodo-2-methyl-benzene (0.15 g, 0.69 mmol), and 1-Difluoromethoxy-4-ethynyl-benzene (0.116 g, 0.69 mmol), and was obtained as a light brown oil, (0.141 g, 79%), identified by NMR and mass spectral analyses. MS (EI+): 258 (M+).

Quelle