Reaktion #2320119

ord-b16965b79860415e9f91c2e53d4a853a

Reaktionsgleichung

FC(F)(F)c1ccc(Cl)c(I)c1
4-chloro-3-iodobenzotrifluoride
CCCN1CCC(=O)CC1
1-propyl-4-piperidone
CCCN1CCC(O)(c2cc(C(F)(F)F)ccc2Cl)CC1
4-(2-Chloro-5-trifluoromethyl-phenyl)-1-propyl-piperidin-4-ol

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Sonstigethe titled compound was recovered by the procedure
  2. 2
    Sonstigedescribed in Preparation 4, MS m/z (rel. intensity, 70 eV)) 321 (M+, 8), 294 (38), 292, (bp), 274 (52), 56 (35)

Vorschrift

Beginning with 4-chloro-3-iodobenzotrifluoride and 1-propyl-4-piperidone, the titled compound was recovered by the procedure described in Preparation 4, MS m/z (rel. intensity, 70 eV)) 321 (M+, 8), 294 (38), 292, (bp), 274 (52), 56 (35).

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: USRE041315E1uspto-grants-2010_05