Reaktion #2303545

ord-f981d22908d1432f81f1432a37e1564f

Reaktionsgleichung

C#CC1(OC(C)=O)CCCCC1
1-acetoxy-1-ethynylcyclohexane
C#CC1(OC(C)=O)CCCCC1
1-Acetoxy-1-ethynylcyclohexane
CN.CO
methylamine methanol
→
C#CC1(NC)CCCCC1
1-Ethynyl-N-methylcyclohexylamine

Edukte

C#CC1(OC(C)=O)CCCCC1
1-acetoxy-1-ethynylcyclohexane
C#CC1(OC(C)=O)CCCCC1
1-Acetoxy-1-ethynylcyclohexane
CN.CO
methylamine methanol

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

This was synthesized in the same manner as in Production Example 18 except that 1-acetoxy-1-ethynylcyclohexane (Production Example 17) and a 40% methylamine/methanol solution were used.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07112593B2uspto-grants-2006_09