Reaktion #2298631

Reaktionsgleichung

2-ethyl-4-methyl-1,6-dihydro-6-pyrimidone

4-[2-bromoethoxy]benzaldehyde

NaH

→

title compound

Ausbeute 42.0%

4-[2-[2-Ethyl-4-methyl-6-oxo-1,6-dihydro-1-pyrimidinyl]ethoxy]benzaldehyde

Ausbeute 42.0%

Reaktionsbedingungen

Vorschrift

The title compound (1.7 g, 42%) was prepared from 2-ethyl-4-methyl-1,6-dihydro-6-pyrimidone (2.0 g, 14.49 mmol), 4-[2-bromoethoxy]benzaldehyde (332 g, 14.19 mmol). LIBr (2.9 g, 33.33 mmol) and NaH (0.45 g, 18.84 mmol) as base, by a similar procedure to that described in preparation 1.

Quelle