Reaktion #2204035

Reaktionsgleichung

sulfuric acid

bis(dimethylamino)dichloromethane

→

bis(dimethylamino)chlorocarbenium hydrogensulfate

Lösungsmittel

water

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeAll volatile compounds are removed under reduced pressure (7.0 Pa)

Vorschrift

3.24 g (33 mmol) of sulfuric acid are added with stirring and ice-cooling to a solution of 5.65 g (33.0 mmol) of bis(dimethylamino)dichloromethane in 30 ml of water. The reaction mixture is warmed to room temperature. All volatile compounds are removed under reduced pressure (7.0 Pa), giving 7.68 g of highly viscous bis(dimethylamino)chlorocarbenium hydrogensulfate, corresponding to a virtually quantitative yield.

Quelle