Reaktion #2203502

ord-dfcf72f84c92443d9ac4e09f69da41d2

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared (0.351 g, 77%) following the general procedure of Example 390 as a white solid, hydrochloride salt from [7-(2,6-dichlorophenyl)-2,3-dihydro-1-benzofuran-2-yl]methyl 4-methylbenzenesulfonate (0.595 g, 1.324 mmol) and methylamine (1.86 g, 60.0 mmol). 190-192 mp ° C.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07435837B2uspto-grants-2008_10