Reaktion #219270

Reaktionsgleichung

1-octene

formic acid

H2O2

→

1,2-Octanediol

Lösungsmittel

ethanol

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe main fraction obtained after the workup
2. 2
   workup.DISTILLATIONby distillation

Vorschrift

314 g (2.80 mol) of 1-octene were reacted with 330 g (7.17 mol) of formic acid and 232 g (3.41 mol) of a 50% strength aqueous H2O2 solution in accordance with Example 4. 575 g of ethanol were employed for the Marlon AS3 acid-catalyzed transesterification, and the main fraction obtained after the workup by distillation was >99.5% pure, virtually odorless 1,2-octanediol.

Quelle