Reaktion #2186187

ord-c9710f0f62934fee89b19dd2f513a20e

Reaktionsgleichung

Cc1ccc(S(=O)c2ccc(C)cc2)cc1
bis(4-methylphenyl)sulfoxide
Cc1ccc(Cl)cc1
4-chlorotoluene
Cc1ccc([S+](c2ccc(C)cc2)c2ccc(C)cc2)cc1.[Cl-]
tris(4-methylphenyl)sulfonium chloride

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    SonstigeThe target compound was obtained
  2. 2
    Sonstigethe procedure of Synthesis Example 1 aside
  3. 3
    Sonstigein Synthesis Example 1
  4. 4
    Extraktionfor extraction

Vorschrift

The target compound was obtained by following the procedure of Synthesis Example 1 aside from using bis(4-methylphenyl)sulfoxide instead of the diphenyl sulfoxide and 4-chlorotoluene instead of the chlorobenzene in Synthesis Example 1, and increasing the amount of water for extraction.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07569324B2uspto-grants-2009_08