Reaktion #217697

ord-1026c601dab64f779845376f2680b9b8

Reaktionsgleichung

CC(=O)Nc1ccc(S(=O)(=O)[O-])c2c1C(=O)/C(=N/Nc1ccc(N=Nc3ccc(S(=O)(=O)[O-])cc3)c3ccc(S(=O)(=O)[O-])cc13)C(S(=O)(=O)[O-])=C2.[Na+].[Na+].[Na+].[Na+]
C.I. Food Black-1
CCNc1cc2oc3cc(=[NH+]CC)c(C)cc-3c(-c3ccccc3C(=O)OCC)c2cc1C.[Cl-]
C.I. Basic Red-1
CN(C)c1ccc(C(=C2C=CC(=[N+](C)C)C=C2)c2ccccc2Cl)cc1.[Cl-]
C.I. Basic Blue-1
CCN(CCCl)c1ccc(C=CC2=[N+](C)c3ccccc3C2(C)C)c(C)c1.[Cl-]
C.I. Basic Violet-7
→
CCN(CC)c1ccc2nc3ccc(NN=C4C=CC(=O)C=C4)cc3[n+](-c3ccccc3)c2c1.[Cl-]
C.I. Basic Black-2

Edukte

CC(=O)Nc1ccc(S(=O)(=O)[O-])c2c1C(=O)/C(=N/Nc1ccc(N=Nc3ccc(S(=O)(=O)[O-])cc3)c3ccc(S(=O)(=O)[O-])cc13)C(S(=O)(=O)[O-])=C2.[Na+].[Na+].[Na+].[Na+]
C.I. Food Black-1
CCNc1cc2oc3cc(=[NH+]CC)c(C)cc-3c(-c3ccccc3C(=O)OCC)c2cc1C.[Cl-]
C.I. Basic Red-1
CN(C)c1ccc(C(=C2C=CC(=[N+](C)C)C=C2)c2ccccc2Cl)cc1.[Cl-]
C.I. Basic Blue-1
CCN(CCCl)c1ccc(C=CC2=[N+](C)c3ccccc3C2(C)C)c(C)c1.[Cl-]
C.I. Basic Violet-7

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

C.I. Basic Red-1, -2, -9, -12, -13, -14, -27; C.I. Basic Blue-1, -3, -5, -7, -9, -24, -25, -26, -28, -29; C.I. Basic Violet-7, -14, -27; C.I. Food Black-1, -2.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07381759B2uspto-grants-2008_06