Reaktion #217480

Reaktionsgleichung

2-acetylnaphthalene

ethyl heptafluorobutyrate

→

4,4,5,5,6,6,6-Heptafluoro-1-(2-naphthyl)-1,3-hexanedione

Reaktionsbedingungen

Aufarbeitung

1. 1
   SonstigeThe compound was synthesized
2. 2
   SonstigeThe product was crystallized from petroleum ether

Vorschrift

The compound was synthesized according to example 1 using 2-acetylnaphthalene and ethyl heptafluorobutyrate as starting materials. The product was crystallized from petroleum ether. 1H NMR (CDCl3): 6.76 (s, 1 H); 7.57-7.66 (m, 2H); 7.90 (bd, 1 H); 7.93-7.94 (m, 2H); 7.98 (bd, 1 H); 8.53 (s, 1H). IR (film): 1602 (C═O); 1232 (C—F).

Quelle