Reaktion #2167452

ord-9198f0dd25f74e95809a03a95843d699

Reaktionsgleichung

C=C(C(=O)[O-])C1C[C@H]2CC[C@@]1(C)C2(C)C
isobornyl acrylate
C=CC(=O)OC
methyl acrylate
C=CC(=O)O
acrylic acid
CCCCCCCCCC(C)C
isododecane
CCCCC(CC)C(=O)OOC(C)(C)CCC(C)(C)OOC(=O)C(CC)CCCC
2,5-bis(2-ethylhexanoylperoxy)-2,5-dimethylhexane
→
C=C(C(=O)[O-])C1C[C@H]2CC[C@@]1(C)C2(C)C.C=CC(=O)O.C=CC(=O)OC
isobornyl acrylate acrylic acid methyl acrylate

Edukte

C=C(C(=O)[O-])C1C[C@H]2CC[C@@]1(C)C2(C)C
isobornyl acrylate
C=CC(=O)OC
methyl acrylate
C=CC(=O)O
acrylic acid
CCCCCCCCCC(C)C
isododecane
CCCCC(CC)C(=O)OOC(C)(C)CCC(C)(C)OOC(=O)C(CC)CCCC
2,5-bis(2-ethylhexanoylperoxy)-2,5-dimethylhexane

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

18 g of isobornyl acrylate, 71.1 g of methyl acrylate, 0.9 g of acrylic acid, 90 g of isododecane and 1.2 g of 2,5-bis(2-ethylhexanoylperoxy)-2,5-dimethylhexane were then introduced into the above mixture, still at 90° C. and over 1 hour.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07932324B2uspto-grants-2011_04