Reaktion #216473

ord-f9da0c90db074d1ea1146f7dfc39580d

Reaktionsgleichung

C#CCOCCC(=O)O
3-(prop-2-ynyloxy)propionic acid
CC(C)(C)C1(CO)COC1
3-t-butyl-3hydroxymethyloxetane
→
C#CCOCCC12OCC(C(C)(C)C)(CO1)CO2
4-t-Butyl-1-[2-(prop-2-ynyloxy)ethyl]-2,6,7-trioxabicyclo[2.2,2]octane

Edukte

C#CCOCCC(=O)O
3-(prop-2-ynyloxy)propionic acid
CC(C)(C)C1(CO)COC1
3-t-butyl-3hydroxymethyloxetane

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

4-t-Butyl-1-[2-(prop-2-ynyloxy)ethyl]-2,6,7-trioxabicyclo[2.2,2]octane was prepared from 3-(prop-2-ynyloxy)propionic acid and 3-t-butyl-3hydroxymethyloxetane using methodology described in Example I.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05466710uspto-grants-1995_11