Reaktion #2143

ord-7999045b166a4c6fb3a5b43a4772dfa0

Reaktionsgleichung

Cn1c(=O)c2[nH]cnc2n(C)c1=O.[Na]
1,3-dimethyl-xanthine sodium salt
CP(C)(=O)CCCCCl
4-chlorobutyldimethylphosphine oxide
→
Cn1c(=O)c2c(ncn2CCCCP(C)(C)=O)n(C)c1=O
[4-(1,3-Dimethylxanthin-7-yl)butyl]dimethylphosphine Oxide

Edukte

Cn1c(=O)c2[nH]cnc2n(C)c1=O.[Na]
1,3-dimethyl-xanthine sodium salt
CP(C)(=O)CCCCCl
4-chlorobutyldimethylphosphine oxide

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title substance was prepared from 10.1 g (0.05 mol) of 1,3-dimethyl-xanthine sodium salt and 4-chlorobutyldimethylphosphine oxide analogously to Example 63.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728686uspto-grants-1998_03