Reaktion #214162

ord-25c9c6c8c5294111bda856bf486330e4

Reaktionsgleichung

COC(=N)C(Nc1ccc(Cl)cc1)C(C)C
methyl 2-(4-chlorophenylamino)-3-methylbutanimidate
OCc1cccc(Oc2ccccc2)c1
3-phenoxybenzyl alcohol
CC(C)C(Nc1ccc(Cl)cc1)C(=N)OCc1cccc(Oc2ccccc2)c1
3-phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate

Lösungsmittel

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

A solution of 2.25 g (10 mmol) of methyl 2-(4-chlorophenylamino)-3-methylbutanimidate and 4.00 g (20 mmol) of 3-phenoxybenzyl alcohol is heated with continuous removal of methanol. Upon cessation of methanol evolution, there is obtained an oil, 3-phenoxybenzyl 2-(4-chlorophenylamino)-3-methylbutanimidate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US04254264uspto-grants-1981_03