Reaktion #2139926
ord-30ba1818977d4670a24a24a0170e33ea
Reaktionsgleichung
Ethyl vinyl ether
benzyl alcohol
→
benzyl vinyl ether
Reagenzien
Reaktionsbedingungen
Detaillierte Bedingungen
See reaction.notes.procedure_details.
Aufarbeitung
- 1ExtraktionThe reaction mixture was extracted with ethyl acetate
- 2Extraktionthe ethyl acetate extract
- 3Waschenwas washed with water
- 4workup.DISTILLATIONfollowed by distillation in vacuo
Vorschrift
Ethyl vinyl ether was mixed in benzyl alcohol, to which was then added mercury acetate, and the mixture was stirred at room temperature for 12 hours. The reaction mixture was extracted with ethyl acetate and the ethyl acetate extract was washed with water, followed by distillation in vacuo to obtain benzyl vinyl ether.