Reaktion #2136

ord-97646f4f01d04c408248a374735fff7f

Reaktionsgleichung

CCOCn1cnc2c1c(=O)[nH]c(=O)n2CC
7-ethoxymethyl-3-ethylxanthine
CCOP(=O)(CCCCCl)OCC
diethyl 4-chlorobutanephosphonate
→
CCOCn1cnc2c1c(=O)n(CCCCP(=O)(OCC)OCC)c(=O)n2CC
Diethyl [4-(7-ethoxymethyl-3-ethylxanthin-1-yl)butyl]phosphonate

Edukte

—
0.01
CCOCn1cnc2c1c(=O)[nH]c(=O)n2CC
7-ethoxymethyl-3-ethylxanthine
CCOP(=O)(CCCCCl)OCC
diethyl 4-chlorobutanephosphonate

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title substance was prepared from 0.01 5 mol of 7-ethoxymethyl-3-ethylxanthine and 0.017 mol of diethyl 4-chlorobutanephosphonate analogously to 53.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US05728686uspto-grants-1998_03