Reaktion #2122479

Reaktionsgleichung

Sodium bis(2-ethylhexyl)sulfosuccinate

AgNO3

→

Silver Bis[2-Ethylhexyl]Sulfosuccinate

Lösungsmittel

diethylether

Reaktionsbedingungen

Aufarbeitung

1. 1
   Sonstigethe aqueous phase was decanted
2. 2
   WaschenThe ether solution is then washed twice with deionized water
3. 3
   SonstigeThe aqueous phase is decanted
4. 4
   Sonstigeevaporation
5. 5
   SonstigeThe remaining paste is dried in a vacuum oven at 25-50° C.
6. 6
   Sonstigea yield in excess of 90%
7. 7
   Sonstigeis obtained

Vorschrift

Sodium bis(2-ethylhexyl)sulfosuccinate (NaAOT) is obtained from Fisher. 10 g NaAOT is dissolved in 100 mL diethylether and combined with an equal volume of 0.1 M aqueous AgNO3 in a separatory flask. The mixture is shaken and the aqueous phase was decanted. Two additional 100 mL volumes of 0.1 M AgNO3 are similarly ion exchanged with the ether solution. The ether solution is then washed twice with deionized water. The aqueous phase is decanted and the ether phase is reduced to a paste using rotary evaporation. The remaining paste is dried in a vacuum oven at 25-50° C., and a yield in excess of 90% is obtained.

Quelle