Reaktion #2075714

ord-9a9f0a1470984ce2842aab81852b12a4

Reaktionsgleichung

ClOCl.[Zr]
zirconium oxychloride
O=S(=O)([O-])[O-].[Na+].[Na+]
sodium sulfate
Cl
hydrochloric acid
→
O=S(=O)([O-])[O-].O=S(=O)([O-])[O-].[Zr+4]
zirconium sulfate

Edukte

ClOCl.[Zr]
zirconium oxychloride
O=S(=O)([O-])[O-].[Na+].[Na+]
sodium sulfate
Cl
hydrochloric acid

Reagenzien

Keine

Reaktionsbedingungen

Temperatur
75°CELSIUS
Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    Temperaturmaintained for 1 hour to age

Vorschrift

625 g of a 16% (ZrO2 conversion) zirconium oxychloride solution at room temperature was added to 237 g of a 25% sodium sulfate solution. After addition of hydrochloric acid to achieve a free acid concentration of 1.5 N, this was heated to 75° C. and maintained for 1 hour to age while producing basic zirconium sulfate.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US07642210B2uspto-grants-2010_01