Reaktion #2063345

ord-e8d1272caf4a47d58cc0af2e8c2488bc

Reaktionsgleichung

Oc1cc2ccc(Br)cc2cc1C12CC3CC(CC(C3)C1)C2
3-(1-adamantyl)-6-bromo-2-naphthol
CCCCCCCBr
1-bromoheptane
CCCCCCCOc1cc2ccc(Br)cc2cc1C12CC3CC(CC(C3)C1)C2
7-(1-adamantyl)-6-heptyloxy-2-bromonaphthalene
Ausbeute 79.0%

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

Following the procedure of Example 8(b), but reacting 3.4 g (9.5 mmol) of 3-(1-adamantyl)-6-bromo-2-naphthol with 2.05 g (11.4 mmol) of 1-bromoheptane, 3.4 g (79%) of 7-(1-adamantyl)-6-heptyloxy-2-bromonaphthalene were obtained.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06225328B1uspto-grants-2001_05