Reaktion #2063055

Reaktionsgleichung

chlorobenzene

sodium carbonate

styrene

propylene carbonate

→

stilbene

Lösungsmittel

diethyl ether

Reaktionsbedingungen

Aufarbeitung

1. 1
   workup.ADDITIONis added
2. 2
   Filtrationthe mixture is filtered

Vorschrift

Under argon, a solution containing 122 mg of chlorobenzene, 229 mg of sodium carbonate, 141 mg of styrene and 1 ml of propylene carbonate stabilized colloid solution with a palladium content of 4.023 mg is heated at 155° C. with stirring in a sealed vessel for 65 h. At the end of the reaction, 2 ml of diethyl ether is added, and the mixture is filtered. The yield of desired product as determined by GC is 34%.

Quelle