Reaktion #2040544

Reaktionsgleichung

hydrogen

6-decanoyl-1,2,3,4-tetrahydro-2-naphthalenecarboxylic acid benzyl ester

→

6-decanoyl-1,2,3,4-tetrahydro-2-naphthalenecarboxylic acid

Ausbeute 111.1%

Lösungsmittel

THF

Reaktionsbedingungen

Aufarbeitung

1. 1
   FiltrationThe reaction mixture was filtered
2. 2
   Einengenby concentrating the filtrate

Vorschrift

50 mL of a THF solution containing 3.79 g (8.69 mmol) of 6-decanoyl-1,2,3,4-tetrahydro-2-naphthalenecarboxylic acid benzyl ester and 0.43 g of 5% palladium/carbon was placed in a hydrogen atmosphere, using a baloon, and was stirred at room temperature for 24 hours. The reaction mixture was filtered and by concentrating the filtrate, there was obtained 3.19 g of 6-decanoyl-1,2,3,4-tetrahydro-2-naphthalenecarboxylic acid. The yield was 100%.

Quelle