Reaktion #2039989

Reaktionsgleichung

Hydrochloric acid

[2-[[N-[2-(diethylamino)ethyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide

→

aimed compound

[2-[[N-[2-(Diethylamino)ethyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide hydrochloride

Lösungsmittel

ethyl acetate

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenthe reaction mixture was concentrated
2. 2
   SonstigeThe residue was recrystallized from ethyl acetate-ethanol mixed solvent

Vorschrift

4N Hydrochloric acid--ethyl acetate solution (0.20 ml) was added to a solution of [2-[[N-[2-(diethylamino)ethyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.42 g) in ethyl acetate (5 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.35 g of the aimed compound as white crystals.

Quelle