Reaktion #2039987

Reaktionsgleichung

Hydrochloric acid

[2-[[N-(2-Aminoethyl)carbamoyloxy]methyl]phenyl]-N-octadecylformamide

→

aimed compound

[2-[[N-(2-Aminoethyl)carbamoyloxy]methyl]phenyl]-N-octadecylformamide hydrochloride

Lösungsmittel

ethyl acetate

ethanol

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenthe reaction mixture was concentrated
2. 2
   SonstigeThe residue was recrystallized from ethyl acetate-ethanol mixed solvent

Vorschrift

4N Hydrochloric acid--ethyl acetate solution (0.30 ml) was added to a solution of [2-[[N-(2-Aminoethyl)carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.33 g) in a mixture of ethyl acetate (10 ml) and ethanol (2 ml) at room temperature. After being stirred for 10 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate-ethanol mixed solvent, thereby yielding 0.30 g of the aimed compound as white crystals.

Quelle