Reaktion #2039978

Reaktionsgleichung

Hydrochloric acid

[2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-tetradecylformamide

→

aimed compound

[2-[[N-[3-(Dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N -tetradecylformamide hydrochloride

Lösungsmittel

ethyl acetate

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Einengenthe reaction mixture was concentrated
2. 2
   SonstigeThe residue was recrystallized from ethyl acetate

Vorschrift

4N Hydrochloric acid--ethyl acetate solution (0.12 ml) was added to a solution of [2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-tetradecylformamide (0.200 g) in ethyl acetate (2 ml) at room temperature. After being stirred for 15 minutes, the reaction mixture was concentrated. The residue was recrystallized from ethyl acetate, thereby yielding 0.197 g of the aimed compound as white crystals.

Quelle