Reaktion #2039976

Reaktionsgleichung

Hydrochloric acid

[2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide

ethanol

→

aimed compound

[2-[[N-[3-(Dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide hydrochloride

Lösungsmittel

ethyl acetate

ethyl acetate

Reaktionsbedingungen

Aufarbeitung

1. 1
   Temperaturwhile being cooled with ice
2. 2
   Einengenthe solution was concentrated
3. 3
   SonstigeThe residue was recrystallized from ethyl acetate

Vorschrift

4N Hydrochloric acid--ethyl acetate solution (0.19 ml) was added to a solution of [2-[[N-[3-(dimethylamino)propyl]carbamoyloxy]methyl]phenyl]-N-octadecylformamide (0.20 g) in ethyl acetate (4 ml) while being cooled with ice. After being stirred for 10 minutes, the deposited crystals were dissolved with ethanol and the solution was concentrated. The residue was recrystallized from ethyl acetate, thereby yielding 0.21 g of the aimed compound as white crystals.

Quelle