Reaktion #2015099

Reaktionsgleichung

2-chloro-4-(3,4-dichloro-phenyl)-6-methyl-pyrimidine

3-bromo-benzene-boronic acid

→

title compound

2-(3-Bromo-phenyl)-4-(3,4-dichloro-phenyl)-6-methyl-pyrimidine

Reaktionsbedingungen

Vorschrift

The title compound was prepared from 2-chloro-4-(3,4-dichloro-phenyl)-6-methyl-pyrimidine (example A.41) (0.4 g, 0.5 mmol) and commercially available 3-bromo-benzene-boronic acid (0.38 g, 1.89 mmol) according to the general procedure IVb. Obtained as an orange solid (0.23 g, 40%). MS (ISP) 394.9 [(M+H)+]; mp 132.5° C.

Quelle