Reaktion #1980469

ord-2a160cbe23eb4e69906446ff1bb5ba2f

Reaktionsgleichung

Cc1ccc(Br)cc1
4-bromotoluene
O=C1CCC2(CC1)OCCO2
1,4-dioxa-spiro[4.5]decan-8-one
→
Cc1ccc(C2(O)CCC3(CC2)OCCO3)cc1
title compound
Cc1ccc(C2(O)CCC3(CC2)OCCO3)cc1
8-p-Tolyl-1,4-dioxa-spiro[4.5]decan-8-ol

Edukte

Cc1ccc(Br)cc1
4-bromotoluene
O=C1CCC2(CC1)OCCO2
1,4-dioxa-spiro[4.5]decan-8-one

Reagenzien

Keine

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Vorschrift

The title compound was prepared as a white solid from 4-bromotoluene (Aldrich) and 1,4-dioxa-spiro[4.5]decan-8-one using the procedure described in Step A of Example 1.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US08513229B2uspto-grants-2013_08