Reaktion #1973963

Reaktionsgleichung

3,4-dinitroaniline

methanesulfonyl chloride

pyridine

→

title compound

N-(3,4-dinitrophenyl)methanesulfonamide

Lösungsmittel

CH2Cl2

Reaktionsbedingungen

Aufarbeitung

1. 1
   EinengenMixture was concentrated under vacuum

Vorschrift

A mixture of 3,4-dinitroaniline (5.27 g, 28.8 mmol), methanesulfonyl chloride (3.36 mL, 43.1 mmol) and pyridine (5.82 mL, 71.9 mmol) in CH2Cl2 (100 mL) was stirred for 24 h. Mixture was concentrated under vacuum to provide a crude semi-solid title compound that was used without further purification.

Quelle