Reaktion #1946553

ord-4c0b174462974ac89e2b7c1c36a908e1

Reaktionsgleichung

CCCCCCCCCCCC(=O)N(C)CC(=O)O
N-lauroylsarcosine
O=S(=O)(O)O
sulfuric acid
→
CCCCCCCCCCCC(=O)N(C)CC(=O)OCCCC
N-lauroylsarcosine butyl ester

Edukte

CCCCCCCCCCCC(=O)N(C)CC(=O)O
N-lauroylsarcosine
O=S(=O)(O)O
sulfuric acid

Reagenzien

Keine

Lösungsmittel

CCCCO
1-butanol

Reaktionsbedingungen

Detaillierte Bedingungen
See reaction.notes.procedure_details.

Aufarbeitung

  1. 1
    TemperaturThe mixture was heated
  2. 2
    Temperaturunder reflux for reaction for 6 hours

Vorschrift

One hundred and thirty-five point five(135.5) grams of N-lauroylsarcosine (ex. Kawaken Fine Chemicals Co., Ltd.) and 200 ml of 1-butanol were charged into a 500-milliliter flask. Further, 4.99 g of conc. sulfuric acid were added as the catalyst. The mixture was heated under reflux for reaction for 6 hours.

Quelle

DOI: 10.6084/m9.figshare.5104873.v1Patent: US06528068B1uspto-grants-2003_03